Analytical methods for Challenge11

Instrument: LC-IT-TOF (Shimadzu)
Ion source: ESI, negative ion mode
Sample Introduction: Infusion
Nebulizer gas: 1.5 L/min
CDL: 200 C
Heat block: 200 C
MS/MS CID gas: Ar 50%
MS/MS CID energy: 80%
q: 0.210 (37.5 kHz)